preview

Potassium Trisoxalatoferrate Lab Report

Good Essays

Abstract By using the green salt synthesis, we obtained Introduction When it comes to using inorganic compounds, such as salts, they contain a complex ion. A complex ion has a central metal ion, to which is then bonded with a neutral molecule that forms ligands. In this experiment, potassium trisoxalatoferrate(III) and potassium ferrioxalate will take part in purifying the product using recrystallization. A pH titration will be used to analyze the mass percent of potassium and iron, meanwhile, the oxidation-reduction titration will be used in order to figure out the mass percent oxalate in the finalized purified product. Once the results of the two percentages are calculated, one must compare them to the theoretical values to indicate …show more content…

Product was rinsed/washed with separate 5 mL portions of ice-cold ethanol. Appearance was recorded of the solid and filtrate before liquid was discarded. Product was dried for 24 hours by being placed in the dark. The mass of the dried product was determined and percent yield was calculated. Part II: Characterization of the Green Salt Observing Photoactivity of the Dissolved Complex Ion Approximately 0.2 g of green salt was transferred in a beaker and dissolved in 50 mL of 1 M H2SO4. One-half of the solution was poured in another beaker and placed in the sunlight, meanwhile, the other half was placed in a cabinet with complete darkness and isolation. Color of both solutions were obtained after 0, 5, 15, and 30 minutes. Each solution was tested for presence of Fe3+ with adding 2 drops of SCN- solution. B. Experimentally Determining Mass% Water Two hot and dry vials were brought to room temperature. Each vial was weighed on a balance to the nearest 0.001 g. 0.9xx g was weighed of the green salt into each vial. Each vial was placed in a 50 mL beaker and initialed with partners names. Samples were heated in the oven for 2

Get Access