A scientist wishes to measure the concentration of methyl benzoate in a plant stream by gas chromatography. He prepares a sample of butyl benzoate to use as an internal standard. The results of a preliminary run, which used a solution known to contain 1.31 mg/mL of methyl benzoate (peak A) and 1.44 mg/mL of butyl benzoate (peak B), are shown. The area of peak A is determined to be 352 and the area of peak B is determined to be 395 measured in arbitrary units by the computer. To measure the sample, 1.00 mL of a standard sample of butyl benzoate containing 2.21 mg/ml. is mixed with 1.00 mL of the plant stream material. Analysis of the mixture gave a peak area of 473 for peak A and 421 for peak B. What is the concentration of methyl benzoate in the plant stream? Detector Response 10 Time (min) 5 15
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- A scientist wishes to measure the concentration of methyl benzoate in a plant stream by gas chromatography. He prepares a sample of butyl benzoate to use as an internal standard. The ic results of a preliminary run, which used a solution known to contain 1.37 mg/mL of methyl benzoate (peak A) and 1.51 mg/mL of butyl benzoate (peak B), are shown. The area of peak A is determined to be 301 and the area of peak B is determined to be 349 measured in arbitrary units by the computer. To measure the sample, 1.00 mL of a standard sample of butyl benzoate containing 2.41 mg/mL is mixed with 1.00 mL of the plant stream material. Analysis of the mixture gave a 10 Time (min) 15 peak area of 499 for peak A and 417 for peak B. What is the concentration of methyl benzoate in the plant stream? methyl benzoate concentration: mg/mL Detector ResponseA scientist wishes to measure the concentration of methyl benzoate in a plant stream by gas chromatography. He prepares a sample of butyl benzoate to use as an internal standard. The results of a preliminary run, which used a solution known to contain 1.37 mg/mL of methyl benzoate (peak A) and 1.51 mg/mL of butyl benzoate (peak B), are shown. The area of peak A is determined to be 301 and the area of peak B is determined to be 349 measured in arbitrary units by the computer. To measure the sample, 1.00 mL of a standard sample of butyl benzoate containing 2.41 mg/mL is mixed with 1.00 mL of the plant stream material. Analysis of the mixture gave a 10 Time (min) 15 peak area of 499 for peak A and 417 for peak B. What is the concentration of methyl benzoate in the plant stream? methyl benzoate concentration: mg/mL Detector ResponseA scientist wishes to measure the concentration of methyl benzoate in a plant stream by gas chromatography. He prepares a sample of butyl benzoate to use as an internal standard. The results of a preliminary run, which used a solution known to contain 1.37 mg/mL of methyl benzoate (peak A) and 1.51 mg/mL of butyl benzoate (peak B), are shown. The area of peak A is determined to be 3.40×102 and the area of peak B is determined to be 398 measured in arbitrary units by the computer. To measure the sample, 1.00 mL of a standard sample of butyl benzoate containing 2.49 mg/mL is mixed with 1.00 mL of the plant stream material. Analysis of the mixture gave a peak area of 437 for peak A and 415 for peak B. What is the concentration of methyl benzoate in the plant stream?
- A scientist wishes to measure the concentration of methyl benzoate in a plant stream by gas chromatography. He prepares a sample of butyl benzoate to use as an internal standard. The results of a preliminary run, which used a solution known to contain 1.35 mg/mL of methyl B benzoate (peak A) and 1.49 mg/mL of butyl benzoate (peak B), are shown. The area of peak A is determined to be 319 and the area of peak B is determined to be 381 measured in arbitrary units by the computer. To measure the sample, 1.00 mL of a standard sample of butyl benzoate containing 2.27 mg/mL is mixed with 1.00 mL of the plant stream material. Analysis of the mixture gave a peak area of 10 Time (min) 15 465 for peak A and 397 for pcak B. What is the concentration of methyl benzoate in the plant stream? methyl benzoate concentration: mg/mL Detector Response25 ml of pickled brine was taken from an apple pickled with vinegar and diluted to 500 ml, 25 ml of this was taken and acidity was determined with 0.2 N (Factor: 1.05) NaOH. In the main trials, 6.3 ml - 6.5 ml - 6.9 ml, respectively, 0.1 ml base was used in the analysis without using the sample.For example, how many ppm is its acidity?An analysis of city drinking water for total hardness was done by two students in the laboratory and produced the following results (in ppm CaCO3): Student A: 228.3, 226.4, 226.9, 227.1, and 228.6. Student B: 229.5, 226.1, 230.7, 223.8, and 227.5 a. What is the mean?
- TOPIC: Recrystallization Students were tasked to conduct a recrystallization experiment to test the ability of the three newly discovered solvents in their laboratory to purify and separate a mixture containing compounds X and Y. The solubilities of the two compounds in g/50 mL of hot and cold solvents are given in the table. Given the data, if a mixture containing 9.0 g each of X and Y is to be recrystallized from 100 milliliters of the solvents, what is the best solvent to use? Support your answer by doing a schematic diagram for EACH solvent.A simple paper chromatography experiment involved the analysis of the food dyes in lollipop samples. A chocolate-flavored lollipop was dissolved using various solvents and was spotted in the chromatogram (E). Four food dye standards (blue, green, red, and orange) were tested alongside the chocolate-flavored lollipop. The mobile phase used for the analysis was 0.1% NaCl. After the analysis, the resulting chromatogram revealed the separation of three colors, which were attributed to the food dyes indigo carmine (blue), tartrazine (yellow), and erythrosine (red). 10 Ruler is in cm unit в с B C D A E A E BEFORE AFTER Calculate the rf for each dye. Express answers in 3SF. erythrosine: indigocarmine: tartrazine: Which dye is the most polar? Choose.. Which dye is the least polar? Choose...The melting temperature of pure acetylsalicylic acid is 135 degrees Celsius. Based on the results of the melting temperature test, what is the percent purity of your sample of aspirin? Part I Synthesis of Aspirin Mass of salicylic acid used (g) 2.029g Volume of acetic anhydride used (mL) 5ml Mass of acetic anhydride used (vol. × 1.08 g/mL) 5.4g Mass of aspirin synthesized (g) 3.256g Part II Melting Temperature Data Melting temperature (°C) 133°C Part III Salicylic Acid Standard Stock Solution Initial mass of salicylic acid (g) 0.210g Moles of salicylic acid (mol) 0.0147 mol Initial molarity of salicylic acid (M) 0.724 M Part III Beer’s Law Data for Salicylic Acid Standard Solutions Trial Concentration (M) Absorbance 1 10 0.301 2 7.5 0.219 3 5.0 0.163 4 2.5 0.074 Best-fit line equation for the salicylic acid standards Test of the Purity of the…
- Q1. Give three criteria for a good recrystallization solvent. Q2. You want to purify 10 grams of benzoic acid that has been contaminated with 0.2 g of salicylic acid. You are given the following data: Solubility in water at 20 °C Solubility at 100 °C (g/10 ml) Compound (g/10 ml) Benzoic Acid 0.029 0.680 Salicylic Acid 0.680 0.029 0.22 6.67 a) What volume of Boiling water is needed to dissolve the 10 g of benzoic acid? (show calculations) b) How much benzoic acid will crystallize after cooling to 20 °C (show calculations) c) Will any salicylic acid crystals form? Why or why not? (show calculations/ reason for answer) d) What is the maximum amount of benzoic acid that could be recovered in the first crop of this recrystallization? (Show calculations) e) How can you prove the purity and identity of the purified Benzoic acid?1. You begin by measuring 10.00 mg of dye on a precise analytical balance and dissolve the dye in 1.000 1 of water having density 998.25 kg/m³. What is the concentration of the dye in mg/l, kg/m³, mg/kg, and ppm?6.0 mL of cyclohexanol, 8 mL of 85% phosphoric acid, and 10 drops of sulfuric acid are added to a 50-mL round-bottom flask with boiling chips, and the mixture is distilled into an ice-cooled receiver. The distillate is in the form of a colorless bi-phasic mixture. The cyclohexene upper layer is removed from the water layer, and dried over anhydrous calcium chloride. Isolated is cyclohexene as a clear and colorless foul-smelling liquid. Weighing data is given below. Gross mass: 51.24 g Tare mass: 48.04 g Product mass: 3.2g Question: Calculate the theoretical mass of the cyclohexene product, bearing in mind that the cyclohexanol starting material was measured by volume, not by mass (so you must use the density of cyclohexanol to convert milliliters to grams, before calculating the number of moles). Calculate the percent yield of cyclohexene obtained.