draw a well-labeled outline of the resolution process of Resolution of Ibuprofen (2-(4’-isobutylphenyl)-propionic acid) and then fully draw out the specific reactions used in the separation process
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draw a well-labeled outline of the resolution process of Resolution of Ibuprofen (2-(4’-isobutylphenyl)-propionic acid) and then fully draw out the specific reactions used in the separation process
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- WILL HEXANE DISSOLVE fenethylline IN GC-MS?Draw a well labeled outline showing how the resolution of ibuprofen process worked and then fully draw out the specific reactions used in the separation process?A student was trying to determine the identity of an unknown compound. The melting point of the compound was 117-118oC. The student narrowed the possible compound down to the following: Compound Melting Point Range acetanilide 113-115oC fluorene 114-116oC mandelic acid 120-122oC A second student, doing the same experiment as above, found that their melting point was 100-108oC. What is wrong with the student’s melting point? Propose two reasons why the melting point could be incorrect. View keyboard shortcuts
- Please show the steps of the separation of a mixture of methyl phenyl ketone and N-methyl amine and indicate the results observed after each step.In a gas chromatogram, the retention time of compounds A and B are 1.25 min and 1.45 min, respectively. If both of these compounds have similar structures, which of the compounds has a higher boiling point?1. Occasionally, a crossed Cannizzaro reaction is carried out to reduce benzaldehyde derivatives to the corresponding benzyl alcohol, utilizing formaldehyde as the reducing agent. i) Please show the mechanism by which this occurs.
- DEPT-135 DEPT - 90 DEPT - 45 T 200 CDS-03-521 180 4/5 160 140 - H₂CO T 120 75% + 100 ppm U 80 LL 60 40 20 0the Infrared spectroscopy experiment by using(FTIR) to identify the unknow compound from the list : EthanolIsoamyl acetateHexanal1-PropanolAnisaldehydeValerophenoneBenzoic AcidCyclohexanonemethyl iso-butyl ketoneBenzyl alcoholPropionaldehydeBenzaldehydePhenylacetic acid3-methylcyclohexanoneMethanolEthyl acetatePinacolonewhich compound is represented in the picture ?Using the infrared spectra provided assign peaks to the functional groups in (a) 3-nitroacetophenone; (b) 3-aminoacetophenone; (c) 1-(3-nitrophenyl)ethanol; (d) 3-nitrobenzaldehyde; (e) 3-aminobenzaldehyde; (f) 3-nitrobenzylalcohol
- Analyze both IR and NMR spectra ,Identify the unknown (solid sample )? Note: the same unknown is used in the experiment to get both IR and NMR. The list of all the possible organic compounds are as follows: Cumene, 3-Methy-2-butanone, Phenethyl alcohol, Isopropyl Acetate, Ethel benzoate, 3-phenylpropionaldehyde, isobutyl cinnamate, cyclamen aldehyde, Styrallyl acetate, Butyl butyrate, propiophenon, phenylacetylene, Cis-Hexenyl-3-Acetate, Benzyl propionate, 3-(p-ethyl-phenyl)-2,2-dimethyl propionaldehyde, 2-methoxy-4-ethyl-phenol, P-ethylphenol, diphenyl amine, 4-phenyl-3-buten-2-one, Diethyl Terphthalate, glutaric acid, cinnamic acid, P- ethylbenzoic acid, Coumarin, vanillin, (2,2,2-trichloro-1-phenylethyl)acetate, 4-(p-hydroxyphenyl)-2-butanone, 2-ethoxy-5-prop-1-enylphenol, t-butyl-phenol, Thymol, Calone, Syringol, Syringaldehyde. Borderline MP unknowns: Styrallyl alcohol, 1,1-dimethyl-2-phenethyl acetate, 1,1-dimethyl-2-phenyl ethanol.Annotate the NMR spectra. Assign the hydrogens to the structure of methyl 3-nitrobenzoate.3. 'H-NMR interpretation When dissolved in CDC13, phenacetin shows 6 signals. All of the peaks are sharp, except for the signal f not below. Draw the chemical structure of phenacetin, labeling each hydrogen with an alphabetical letter. Make a larger version of the chart below (half or full page), and complete it with the missing information. Explanation of splitting patter 8 (ppm) Letter # H (integration Splitting pattern value) 7.94 f 1 Broad singlet 7.36 e 6.80 d 3.98 с 2.09 b 1.38 a Extra Credit Question 4. Describe/predict how the 'H-NMR spectrum differs for acetaminophen.