Ni(II)-aminopyridine complex was synthesized using a metal-template condensation reaction presented below. Compound C is the target compound, but other Ni complexes can be produced as well as the intermediates of the reaction. Н он H. H2N H2N- Ni(CIO4)2 'N + HN N NP* HN 2 CIO, N NP* HN 2 CIO, N NP* HN 2 CIO," H,O-EIOH reflux H2N. A B C What spectral features would you expect to see in MS and IR to determine whether the synthesis was fully successful/complete?

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
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Chapter14: Applications Of Ultraviolet-visible Molecular Absorption Spectrometry
Section: Chapter Questions
Problem 14.15QAP
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Ni(II)-aminopyridine complex was synthesized using a metal-template condensation reaction presented below.
Compound C is the target compound, but other Ni complexes can be produced as well as the intermediates of the
reaction.
H
Н он
H
H2N
H2N
Ni(CIO,2
'N
+
HN
N Ni2* HN 2 CIO,
N N* HN
2 CIO,
N N2* HN
2 CIO,
H2O-ELOH
reflux
H2N.
A
B
What spectral features would you expect to see in MS and IR to determine whether the synthesis was fully
successful/complete?
Transcribed Image Text:Ni(II)-aminopyridine complex was synthesized using a metal-template condensation reaction presented below. Compound C is the target compound, but other Ni complexes can be produced as well as the intermediates of the reaction. H Н он H H2N H2N Ni(CIO,2 'N + HN N Ni2* HN 2 CIO, N N* HN 2 CIO, N N2* HN 2 CIO, H2O-ELOH reflux H2N. A B What spectral features would you expect to see in MS and IR to determine whether the synthesis was fully successful/complete?
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