Show how you would use extractions with a separatory funnel to separate a mixture of the following compounds: benzoicacid, phenol, benzyl alcohol, aniline

Q: Write a reaction showing how the compound ethanoic propanoic anhydride is prepared.

A: To draw: The formation of ethanoic propanoic anhydride?

Q: A Claisen condensation

A: (a)

Q: The 1H NMR spectra for two esters with molecular formula C8H8O2 are shown next. Which of the esters…

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Q: (b) A compound that contains both hydroxyl and carboxyl groups undergoes intramolecular ester…

A: The lactone formed by intramolecular ester formation is shown as,

Q: Show how you would convert propan-1-ol to the following compounds using tosylateintermediates. You…

A: One of the methods of amination of an alcohol involves the conversion of an alcohol to the tosylate…

Q: Following are structural formulas for phenol and cyclohexanol along with the acid dis- sociation…

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Q: A student was performing an acid-base extraction of a mixture of three compounds. The three…

A: The solution is as follows:

Q: Outline an extraction procedure by which you would separate a mixture of the following three…

A: Step 1 : mixture of compounds is treated with 10% HCl, aniline will go into water layer. water layer…

Q: The following compounds (A-D) are isolated from anise and fennel (as well as various related…

A: compound B orC

Q: 9-Aminofluorene has applications in the structural analysis of proteins and carbohydrates. Write a…

A: The given compounds are 9-aminofluorene and fluorene. In this question, a mixture of 9-aminofluorene…

Q: OH OH H2N Benzoie Acid Biphenyl Benzocaine Phenol benzocaine phenol biphenyl benzoic acid | dissolve…

A: The organic compounds present in the mixture are benzocaine, phenol, biphenyl and benzoic acid.

Q: Acetic acid, salicylic acid, benzoic acid all of them undergo esterification test separately with…

A: When carboxylic acid reacts with alcohol in presence of H2SO4 then ester is formed.  Mechanism : At…

Q: Propose a synthetic route for the following conversion: toluene benzyl (methyl) amine

A: The conversion required: toluene to benzyl methyl amine.

Q: Given this retrosynthetic analysis, propose a synthesis for the antidepressant moclobemide. CI H CI…

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Q: Develop a flow chart to show how you can separate the following two compounds using acid-base…

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Q: A student mixes benzaldehyde with an unknown symmetrical ketone, compound C, in an aqueous sodium…

A: The question is based on the concept of spectroscopy. We have to identify the structure of C &D.

Q: Draw the structure of two esters that will be reduced to propanol and butanol by LiAlH4 (followed by…

A: Since the LiAlH4 reduces the esters into the respective alcohols. And since the ester can have 2…

Q: What generalization trends may be extracted from the following series in terms of solubility with…

A: Acid base reaction is faster than other reaction so Base will react first with an acid. Now in set…

Q: Provide a retrosynthetic analysis and a synthesis of amino acid D, using 3- chlorobenzaldehyde as…

A: Please find the attachment.

Q: Arrange the following in increasing solubility with water Toluene Benzaldehyde Hydroquinone…

A: Solubility of a compound in water depends on the polarity of solute, because water is a polar…

Q: Starting from Benzene, Carbon Dioxide, and any other reagents, how could you prepare…

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Q: Spasmolytol, as its name suggests, is an antispasmodic. Given this retrosynthetic analysis, propose…

A: Spasmolytol  is an antispasmodic drug that used to relieve the pain of involuntary muscle. Salicylic…

Q: A. Reaction with Nitrogen Compounds; Write whether the following aldehydes and ketones are positive…

A: A. The aldehydes and ketones considered are not positive species. But have polarized carbonyl bonds…

Q: . ammoniacal AgNO₃   which will match and quickly differentiate the compounds in the ff:   1.…

A: The question is based on the concept of organic reactions. we have to identify which of the given…

Q: Show the structures that form when Ethyl mesylate reacts with potassium iodide in acetone

A: It is the example of substitution reaction

Q: 6) If you are given a mixture consisting of following 3 compoünds components by solvent extraction…

A: Given three compounds: Cyclopentylamine (A) is basic in nature. 2,4-cyclopentadiene-1-carboxylic…

Q: OMe OMe

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Q: How to separate phenol from a mixture of benzoic acid and phenol by extraction?

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Q: Show the reagent needed to convert butanoic acid to its derivative of i. butanoyl chloride ii.…

A: In chemistry, reagent can be defined as the substance which is used to convert reactant into…

Q: Following is a series of anorexics (appetite suppressants). As you study their structures, you will…

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Q: Match each of the following with the correct answer. v Benzoyl chloride and propan-2-amine A. Butyl…

A: Since you have posted a question with multiple sub-parts, we will solve first three sub-parts for…

Q: Show how to convert cyclopentanone to these compounds. In addition to cyclopentanone, use any other…

A: Reduction reactions the gaining of an electron, a gain of hydrogen, loss of oxygen. Cyclopentanone…

Q: You have learned that ester may be hydrolyzed in aqueous base. Why does a workup using 50ml of 10%…

A: Esters may be hydrolyzed in aqueous bases.

Q: To further exemplify your understanding of acid-base extraction, fill in the following generic chart…

A: We are given 4 different organic compounds are given to separate using acid-base extraction, which…

Q: Provide a stepwise synthesis for benzyl alcohol to benzoic acid (including arrow-pushing mechanisms)…

A: When benzyl alcohol is treated with K2Cr2O7 and c. H2SO4 then sodium benzoate is formed which upon…

Q: Show how to prepare the following aromatic amines by aromatic nitration, followed by reduction. You…

A: The structure of p-bromoaniline is shown below.

Q: Suppose you have a mixture of these three compounds. Devise a chemical procedure based on their…

A: The aromatic nitro compounds are depicted by Ar-NO2 and the nitro substituent deactivates the ring…

Q: the reaction of the phenol nitration, a mixture of o-nitrophenol and p-nitrophenol is formed. The…

A: We will explain melting point

Q: Show how to prepare the following aromatic amines by aromatic nitration, followed by reduction. You…

A: Nitration is chemical process in which nitro group is introduced into an organic compound.

Q: A Student added 1.5 ml of 3 M Methyl Magnesium Bromide to a conical vial containing Benzophenone &…

A: Methyl magnesium bromide acts as a good source of Nucleophile CH3- , thus it carry out nucleophilic…

Q: Write out steps to show how each of the following pairs of compounds can be separated by an…

A: Introduction: Extraction is a process in chemistry in which two or more chemical species can be…

Q: Phenacetin has the structure given below. Write an equation for its preparation starting from…

A: To write the reaction of: Preparation of Phenacetin from 4-ethoxyaniline.

Q: Write out the 3-step arrow pushing mechanism showing how methyl2,2-dimethylpropanoateis hydrolyzed…

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Q: NH CH3 N-benzylacetamide

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Q: Following is a retrosynthetic analysis for the synthesis of the herbicide (S)-Metolachlor from…

A: The retrosynthetic method is used to predict the starting material from product structure by…

Q: Give TWO reagents to prepare cyclopentanone from adipic acid.

A: Adipic acid is dicarboxylic acid and cyclopentanone is ketone. We have to two reagents for…

Analyzing and Predicting Spectroscopic Data

The interaction of electromagnetic radiation with the structure of molecules in the sample and their study is referred spectroscopy. Several spectroscopic methods are used to acquire sample information, and these methods are proved to be accurate, fast, and non-destructive. The information obtained about the content and composition of molecules from these spectroscopic methods is called spectroscopic data.