What makes ethyl acetate a suitable or unsuitable solvent? What concerns would you have if you were to run a column using hexanes as the solvent for the whole column? Come up with an appropriate solvent gradient to get the best separation of all three compounds

Chemistry: An Atoms First Approach
2nd Edition
ISBN:9781305079243
Author:Steven S. Zumdahl, Susan A. Zumdahl
Publisher:Steven S. Zumdahl, Susan A. Zumdahl
Chapter21: Organic And Biological Molecules
Section: Chapter Questions
Problem 103E
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What makes ethyl acetate a suitable or unsuitable solvent?

What concerns would you have if you were to run a column using hexanes as the solvent for the whole column?

Come up with an appropriate solvent gradient to get the best separation of all three compounds
--------
ethyl acetate
· - - - - - - - ·
1:1 hexanes/
ethyl acetate
----
hexanes
Transcribed Image Text:-------- ethyl acetate · - - - - - - - · 1:1 hexanes/ ethyl acetate ---- hexanes
Fe
acetylferrocene
Fe
1,1'-diacetylferrocene
Fe
ferrocene
Transcribed Image Text:Fe acetylferrocene Fe 1,1'-diacetylferrocene Fe ferrocene
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