In the synthesis of Sudan-1, the following precursors were used: Aniline – 0.2 mL β-naphthol – 0.35 g   Experimental data Weight of vial, g 13.1085 Weight of vial + recrystallized product, g 13.4714 Experimental melting point, °C 129-132 Given this data: What is the theoretical yield? What is the percent yield? What is the purity of the dye based on experimental melting point (theoretical is 131-133 °C) Please show solutions and equations

Organic Chemistry
8th Edition
ISBN:9781305580350
Author:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Publisher:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Chapter23: Amines
Section23.6: Reactions With Acids
Problem 23.9P
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In the synthesis of Sudan-1, the following precursors were used:

Aniline – 0.2 mL

β-naphthol – 0.35 g

 

Experimental data

Weight of vial, g

13.1085

Weight of vial + recrystallized product, g

13.4714

Experimental melting point, °C

129-132

Given this data:

  1. What is the theoretical yield?
  2. What is the percent yield?
  3. What is the purity of the dye based on experimental melting point (theoretical is 131-133 °C)

Please show solutions and equations

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