When 10 g of activated carbon is mixed with 1 M 100 ml of acetic acid solution and filtered, a 20 ml sample taken from the filtrate is diluted to 100 ml with distilled water and titrated with 1 N NaOH solution besides the ffindicator, and find the percentage of acetic acid adsorbed as 5 ml of NaOH is consumed. (Masetic acid = 60 gr / mol). %3D e 3:54
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- 5. A 300.0 mg sample containing Na,CO3, NaHCO3 and NaOH and inert material either alone or in some combination was dissolved and titrated with 0.1000 M HCI the titration required 24.41 mL to reach the phenolphthalein endpoint. And an additional 8.67 mL to reach the methyl red endpoint. Determine the composition of the sample and calculate the percent of each titrated component.5. A 300.0 mg sample containing Na,CO3, NaHCO, and NaOH and inert material either alone or in some combination was dissolved and titrated with 0.1000 M HCI the titration required 24.41 ml to reach the phenolphthalein endpoint. And an additional 8.67 mL to reach the methyl red endpoint. Determine the composition of the sample and calculate the percent of each titrated component.An unknown sample containing mixed alkali (NaOH / NaHCO3 / Na2CO3) was analyzed using the double titration method. A 250-mg sample was dissolved in 250-mL CO2 free water. A 20.0-mL aliquot of this sample required 11.3-mL of 0.009125M HCl solution to reach the phenolphthalein endpoint. Another 20.0-mL aliquot of the sample was titrated to the bromocresol green endpoint using 31.1-mL of the standard acid. What is/are the component(s) of the sample? How many mmol of the components are there in the original solid sample?
- 7. Sodium nitrite was assayed by residual titration with 0.1N potassium permanganate and 0.1 N oxalic acid. What is the gram-equivalent weight (gew) of sodium nitrite? (NaNO2=68.99g/mol) NaNO2+ KMnO4 +H2SO4 ® HNO3 + MnSO4 + Na2SO4 + K2SO4 + H2O KMnO4 + H2C2O4 + H2SO4 ® MnSO4 + K2SO4 + CO2 + H2O ㅋA 0.9092-g sample of a wheat flour was ana- lyzed by the Kjeldahl procedure. The ammonia formed was distilled into 50.00 mL of 0.05063 M HCI; a 7.46-mL back-titration with 0.04917 M NAOH was required. Calculate the percent- age of protein in the flour. 9-22.An unknown sample containing mixed alkali (NAOH, NaHCO3, or NazCO3) was analyzed using the double flask method. A 250 mg sample was dissolved in 250 mL CO2 free water. A 20.0 mL aliquot of this sample required 11.3 mL of 0.009125 M HCI solution to reach the phenolphthalein end point. Another 29.0 mL aliquot of the sample was titrated to the bromocresol green endpoint using 31.1 mL of the standard acid. How many millimoles of the components are there in the original solid sample? O 0.28 mmol Na,CO3 O 1.29 mmol NaOH, 0.97 mmol Na2CO3 O 0.103 mmol NaOH, 0.078 mmol NazCO3 O 1.29 mmol Na2CO3, 0.97 mmol NaHCO3 O Cannot be determined
- A 10.00mL sample of alcoholic ethyl acetate was diluted to 100.00 mL. 20.00 mL was aliquoted and mixed with 40.00 mL of 0.04672 M KOH. The resulting mixture was heated for 2 hours. CH3COOC2H5 + OH- → CH3COO- + C2H5OH After cooling, the excess OH was back titrated with 3.41 mL of 0.05042 M H2SO4. Answer the following: Calculate the number of moles of OH- that reacted with ethyl acetate. Calculate the number of moles of ethyl acetate in the 20.00 mL solution. What is the mass of ethyl acetate (FW=88.11 g/mol) in the original 10.00 mL sample?The thiourea in a 1.455-g sample of organic material was extracted into a dilute H2SO4solution and titrated with 37.31 mL of 0.009372 M Hg2+via the reaction4(NH2)2CS + Hg2+ S [(NH2)2CS]4Hg2+Find the percentage of (NH2)2CS (76.12 g/mol) in the sample.A 0.1093-g sample of impure Na2CO3 was analyzed by the Volhard method. After adding 50.00 mL of 0.06911 M AgNO3, the sample was back-titrated with 0.05781 M KSCN, requiring 27.36 mL to reach the endpoint. Report the purity of the Na2CO3 sample. [Ans. 90.9 % (w /w )]
- A 0.2028 g sample of primary standard grade Na2C2O4 (M.M. = 134.00) was dissolved in 100 mL of 1 M H2SO4. The solution required 22.42 mL of the KMnO4 solution to reach the phenolphthalein end point. Titration of the blank (100 mL of 1M H2SO4) required 0.02 mL of the KMnO4 solution. What is the molarity of KMnO4An unknown sample containing mixed alkali (naoh, nahco3, or na2co3) was analyzed using the double flask method. a 250 mg sample was dissolved in 250 ml co2 free water. a 20.0 ml aliquot of this sample required 11.3 ml of 0.009125 m hcl solution to reach the phenolphthalein end point. another 29.0 ml aliquot of the sample was titrated to the bromocresol green endpoint using 31.1 ml of the standard acid. how many millimoles of the components are there in the original solid sampleSuppose that you use 0.75 g of iron in this experiment. What is the minimum volume of 1.5 M CuSO4 solution required a) using eq. (5-1)? Fe(s) + Cu2+(aq) -> Fe2+(aq) + Cu(s) b) using eq. (5-2)? 2Fe(s) + 3Cu2+(aq) -> 2Fe3+(aq) + 3Cu(s)