Trials 1 2 3 Volume of aliquot of standard CaCO, solution 25.00 (ml) 25.00 25.00 Volume of titrant, EDTA (ml) 23.20 23.50 23.34 Titer (mg CaCO,/mL EDTA) Trial 1 Trial 2 Trial 3
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- M 23 (H) Inorganic Analytical Chemistry pard My courses CHEM 23 (H) FS-AY:20-21 Week 4-5: Quantitative Analysis by Gravimetry and Titration Quiz 4 Qu 10 The 500.0-mg sample of impure Na2 CO3 (FM: 105.96) required 22.00 mL of the HCI standard solution (the obtained concentration of HCI from the previous question, problem 5: Titrimetry short answer type) for complete neutralization. ut of 1. Give the balanced chemical equation between the sample, Na2CO3 and the standard, HCI. 2. What is the mass (g) of Na, CO3 in the sample? 3. Calculate the % (w/w) purity of a 500.0-mg sample of impure Na2 CO3 Note: Type your solution here or upload its pic in Jpeg or pdf format. Another option is to send it to me via email (subject: Fam name-Quiz 4) or messenger, privately. Do not forget to box the final answer and write your name. В I 1.MAX OF 15 MINUTES A solution contains NaOH (FM = 40), NaHCO3 (FM = 84), and NazCO; (FM = 106), either alone or in a permissible combination. Titration of a 50 mL portion to a phenolphthalein end point requires 16.3 mL of 0.100 M HCI. A second 50.0-mL aliquot requires 38.2 mL of the HCI when titrated to a bromocresol green end point. %3D %3D What is the % w/w composition of the following? Express answers in two decimal places. If the component is not present, write 0.00 in the answer box. NAOH: NazCO3: NaHCO3: 96Aspirin powder = 0.8110g MW of Aspirin = 180g.mol-1 Volume of 0.5N HCl consumed in back titration = 23.50mL Volume of 0.5N HCl consumed in blank titration = 44.50mL Percent purity (USP/NF) = Aspirin tablets contain NLT 90.0% and NMT 110.0% of the labeled amount of aspirin (C9H8O4) What is the calculated weight (in grams) of pure aspirin?..
- Table A: Standard NaCl used to make primary standard solution Mass of weighing bottle + NaC1 (g) 21.8720 Mass of weighing bottle after transfer (g) 21.772 Mass of NaCl used in solution (g) 0.6948 Purity of NaCl (%) 100.03 Table A: unknow used to make primary standard solution Mass of weighing bottle + unknow (g) 16.8777 Mass of weighing bottle after transfer (g) 16.20010 Mass of unknow used in solution (g) 0.6776 Purity of unknow (%) Table C: Titration of 25.00 mL aliquots of NaCl with AGNO3 Trial 1 Trial 2 Trial 3 Final Burette Reading (mL) 28.29 24.79 25.11 Initial Burette Reading (mL) 4.99 1.49 1.69 Volume Added (mL) 23.30 23.30 23.42 Table C: Titration of 25.00 mL aliquots of unknow with AGNO3 Trial 1 Trial 2 Trial 3 Final Burette Reading (mL) Initial Burette Reading (mL) 23.99 22.45 26.91 2.89 1.25 5.61 Volume Added (mL) 21.10 21.20 21.30Concentration sodium thiosulfate solution used: 0.056 mol L-1 ACCURATE TITRATION VOLUME OF SODIUM THIOSULFATE SOLUTION USED Volume titration 1, (ml) Volume titration 2, (ml) Your Group 15.80 15.75 Group 1 16.05 15.70 Group 2 16.30 16.25 ANALYSIS Average volume used, (mL) Standard deviation Number of moles sodium thiosulfate used, (mol) Number of moles calcium iodate in solution, (mol) Volume of calcium iodate used, (mL) Concentration of saturated calcium iodate solution (mol L-¹) Unrounded value 15.9750 0.26220 Rounded value 15.97 0.262 10.0Given the following data Dissolved Oxygen Titration Data Trial 1 Preparation of titrant 0.4455 g NazS203•5H20 in 50.0 mL water Mass of water sample used (g) 5.21 g Initial mass of Na2S203 soln and Beral pipet(g) 12.40 g Final mass of Na2S203 soln and Beral pipet(g) 12.20 g MW of Na2S203•5H2O 248.11 g/mol MW of NazS203 158.11 g/mol MW of O2 32 g/mol Calculate the following: a) Concentration of Na2S203•5H20 in mol/g c) DO of sample (ppm) Final answer: 3 significant figures
- Concentration sodium thiosulfate solution used: 0.056 mol L-1 ACCURATE TITRATION VOLUME OF SODIUM THIOSULFATE SOLUTION USED Volume titration 1, (mL) Volume titration 2, (mL) Your Group 15.80 15.75 Group 1 16.05 15.70 Group 2 16.30 16.25 ANALYSIS Average volume used, (ml) Standard deviation Number of moles sodium thiosulfate used, (mol) Number of moles calcium iodate in solution, (mol) Volume of calcium iodate used, (mL) Concentration of saturated calcium iodate solution (mol L-¹) Unrounded value 15.9750 0.26220 0.00089400 0.00036700 A Rounded value 15.97 0.262 8.94 x 10-4 10.0 MinimizeIn this double titration experiment determining composition of soda ash, you are given the following data: M HCl titrant: 0.0501 M +/- 0.0507 Mass of soda ash sample, g: 0.2505 ± 2.0e-4 (Analytical Balance) Total volume of Sample Stock, mL: 75 ± 0.05 (100mL graduated cylinder) Volume of Sample Stock Aliquot, mL: 25 ± 0.3 Find the missing information. Show solutions3. sample of pure CaCO3 (MW 100.09) weighing 0.4148 g is dissolved in 1: 1 hydrochloric acid and the solution is diluted to 500 mL in a volumetric flask. A 50.0 –mL aliquot is withdrawn with a pipet and placed in an Erlenmeyer flask. The solution is titrated with 40.34 mL of an EDTA solution using Erichrome Black T indicator. Calculate the molarity of the EDTA solution.
- The mass percent of Fe in an unknown salt sample was determined using both volumetric and gra vimetric titration. Ten determinations using both methods were performed. Volumetric(% of Fe): 24.22, 23.86, 24.07, 24.49, 24.69, 23.71, 24.28, 24.11, 24.26, 24.10 Gravimetric (% of Fe): 24.35, 24.26, 24.10,24.19, 24.18, 24.32, 24.11, 24.33, 24.17, 24.12 a. Do the two methods give similar standard deviations? b. Do the two methods give similar results for the mass percent of Fe at the 95% confidence level?Data Table 3: Complexometric Titration of Soft Water 6ml of water used (1ml of buffer and 5ml of soft water) Hard Water Trial 1 Hard Water Trial 2 Hard Water Trial 3 Initial Syringe Reading (mL) 1ml 1ml 1ml Final Syringe Reading (mL) 77ml 79ml 75ml Volume of EDTA Consumed (mL) .23ml .21ml .25ml Water Hardness ppm CaCO3 (mg/L) Average ppm CaCO3 (mg/L):The buret was filled with 0.100 M HCl solution. Then was transferred in a 25.0 mL of saturated calcium hydroxide solution (2g of calcium hydroxide per 100 ml of water) in two separate E-flasks. Then 2 drops of phenolphthalein was added to each flask Titration data for the determination of solubility and Ksp of calcium hydroxide: Trial 1: Final Buret reading (ml)-19.80; Initial Buret reading (ml)- 13.00; Temperature (Celcius)- 25 Trial 2: Final Buret reading (ml)-26.10; Initial Buret reading (ml)- 19.80; Temperature (Celcius)- 25 Voume of HCl used: Trial 1- 6.80ml; Trial 2- 6.30mL 1. Compute for the moles of H+ used and the moles of OH- present. moles of H+ used = (concentration of HCl) × (volume of HCl used)moles of OH- = moles of H+ used 2. Construct an ICE table for the reaction.3. Calculate the molar solubility (in mol/L) of OH- and Ca2+.4. Determine the solubility of Ca(OH)2 in g/L. (MM of Ca(OH)2 = 74.096 g/mol). 5.…